• 专利标题:   Preparation of graphene-metal composite microwave-absorbing material, involves adding metal salt aqueous solution to graphene oxide, freeze-drying, heating in tubular furnace, and introducing pure nitrogen/hydrogen for reduction reaction.
  • 专利号:   CN107333460-A, CN107333460-B
  • 发明人:   HUO L, DONG Y, GAO Y, SHEN Q, XU J, DENG K
  • 专利权人:   UNIV HEBEI, UNIV HEBEI
  • 国际专利分类:   C09K003/00, H05K009/00
  • 专利详细信息:   CN107333460-A 07 Nov 2017 H05K-009/00 201782 Pages: 13 Chinese
  • 申请详细信息:   CN107333460-A CN10523335 30 Jun 2017
  • 优先权号:   CN10523335

▎ 摘  要

NOVELTY - Preparation of graphene-metal composite microwave-absorbing material, involves dissolving a soluble metal salt in water to obtain a metal salt aqueous solution, adding the metal salt aqueous solution to graphene oxide, freeze-drying to obtain a metal salt/graphene oxide mixture, placing the mixture in a tubular furnace, increasing the furnace inner temperature from room temperature to 250-300 degrees C at 10-15 degrees C/minute, and introducing pure nitrogen or pure hydrogen for reduction reaction. The mass ratio of metal element of the metal salt with respect to graphene oxide is 1-2:10. USE - Preparation of graphene-metal composite microwave-absorbing material (claimed). ADVANTAGE - The method enables environmentally-friendly and economical preparation of graphene-metal composite microwave-absorbing material comprising metal uniformly dispersed in graphene in the form of quantum dots or nanoparticles with a particle size of 2-20 nm, without introduction of impurities. The material has excellent microwave-absorbing capability, and absorption effect with respect to electromagnetic waves of low-high frequency, and achieves 90% microwave attenuation.