• 专利标题:   Preparation of graphene/aluminum composite material involves ultrasonically treating graphene oxide aqueous solution, cooling adding aluminum powder, stirring, carrying out solid liquid separation, freeze drying and thermally reducing.
  • 专利号:   CN105385870-A, CN105385870-B
  • 发明人:   LI X, MENG Y, WANG J, WU H, HOU L
  • 专利权人:   TANGSHAN JIANHUA TECHNOLOGY DEV CO LTD, TANGSHAN JIANHUA TECHNOLOGY DEV CO LTD
  • 国际专利分类:   C22C001/04, C22C001/10, C22C021/00
  • 专利详细信息:   CN105385870-A 09 Mar 2016 C22C-001/04 201646 Pages: 5 English
  • 申请详细信息:   CN105385870-A CN10729890 02 Nov 2015
  • 优先权号:   CN10729890

▎ 摘  要

NOVELTY - The preparation of graphene/aluminum composite material involves ultrasonically treating graphene oxide aqueous solution, uniformly dispersing, allowing to stand, cooling resulting aqueous solution of graphene oxide, adding aluminum powder, stirring to obtain uniform aqueous solution of graphene oxide containing aluminum powder, carrying out centrifugal cryogenic solid liquid separation of obtained aqueous solution, freeze drying to obtain graphene oxide/aluminum composite dry powder, and thermally reducing graphene oxide/aluminum composite dry powder in argon/hydrogen mixed gas. USE - Preparation of graphene/aluminum composite material (claimed). ADVANTAGE - The method enables industrial production of graphene/aluminum composite material by simple, efficient and easy process. The graphene/aluminum composite material has high strength, low thermal expansion coefficient, and enhances specific strength and specific stiffness coefficient. DETAILED DESCRIPTION - The preparation of graphene/aluminum composite material involves ultrasonically treating graphene oxide aqueous solution, uniformly dispersing, allowing to stand, cooling resulting aqueous solution of graphene oxide at 5 degrees C under stirring, adding slowly aluminum powder, stirring, controlling the temperature less than 5 degrees C, stirring speed to 100-1000 rpm and stirring time to 1-2 hours to obtain uniform aqueous solution of graphene oxide containing aluminum powder, carrying out centrifugal cryogenic solid liquid separation of obtained aqueous solution, freeze drying after the separation of cream solid to obtain graphene oxide/aluminum composite dry powder, and thermally reducing graphene oxide/aluminum composite dry powder in argon/hydrogen mixed gas.