• 专利标题:   Preparing controllable graphene aerogel comprises e.g. adding graphene oxide into distilled water, ultrasonically dispersing, dispersing intercalation modifier in solvent, performing ion exchange reaction and freeze drying.
  • 专利号:   CN108147396-A
  • 发明人:   ZHANG C
  • 专利权人:   SHANDONG JIAIXNG ENVIRONMENTAL PROTECTIO
  • 国际专利分类:   C01B032/184, C01B032/198
  • 专利详细信息:   CN108147396-A 12 Jun 2018 C01B-032/184 201843 Pages: 5 Chinese
  • 申请详细信息:   CN108147396-A CN10112796 05 Feb 2018
  • 优先权号:   CN10112796

▎ 摘  要

NOVELTY - Preparing controllable graphene aerogel comprises (i) adding graphene oxide into distilled water and ultrasonically dispersing to obtain graphene oxide dispersion having concentration of 2-12 mg/cm3, where molar ratio between graphene oxide and distilled water is 10:30-200, (ii) dispersing 0.1-40 mmol intercalation modifier in solvent to prepare 5-25 wt.% solution, then adding into graphene oxide dispersion and performing ion exchange reaction at 20-60 degrees C for 2-20 hours to obtain graphene oxide modified solution, and (iii) freeze drying graphene oxide modified solution at -80 to -10 degrees C under pressure of 2-10 MPa or supercritical drying at 100-300 degrees C under pressure of 5-12 MPa to obtain graphene aerogel. USE - The method is useful for preparing controllable graphene aerogel.