• 专利标题:   Silicon dioxide nanosphere/graphene composite material has amorphous silicon dioxide nanospheres closely attached to graphene, where silicon dioxide nanospheres have specific diameter.
  • 专利号:   CN107732211-A
  • 发明人:   YANG Y, GAO Y, LIU J, FANG X
  • 专利权人:   UNIV HEFEI TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/48, H01M004/587
  • 专利详细信息:   CN107732211-A 23 Feb 2018 H01M-004/36 201821 Pages: 9 Chinese
  • 申请详细信息:   CN107732211-A CN10993220 23 Oct 2017
  • 优先权号:   CN10993220

▎ 摘  要

NOVELTY - A silicon dioxide nanosphere/graphene composite material has amorphous silicon dioxide nanospheres closely attached to the graphene. The silicon dioxide nanospheres have a diameter of 150-250 nm. USE - Silicon dioxide nanosphere/graphene composite material. ADVANTAGE - The silicon dioxide nanosphere/graphene composite material can be prepared using inexpensive raw materials in a simple manner. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of silicon dioxide nanosphere/graphene composite material, which involves: (a) weighing 30 ml ethanol and 3 ml deionized water, fully mixing to prepare an ethanol/water mixed solution, adding 30 mg graphite oxide to the ethanol/water mixed solution, then adding 25 mg surfactant sodium dodecylbenzenesulfonate to obtain a mixed reaction liquid (A), placing the mixed reaction liquid (A) in an ice bath at 0 degrees C, and carrying out ultrasonic treatment until the graphite oxide in the mixed reaction solution (A) is completely dissolved to obtain a mixed reaction solution (B); (b) weighing 25 ml tetraethyl orthosilicate, dripping the tetraethyl orthosilicate into the mixed reaction solution (B), then adding 3 mg sodium hydroxide, carrying out ultrasonic treatment for 15 minutes to obtain a mixed reaction solution (C), stirring the mixed reaction solution (C) for 2 hours using a magnetic stirrer, then transferring the fully stirred mixed reaction solution (C) to a 100 ml PTFE reaction kettle liner, and carrying out reaction at a high-temperature of 160 degrees C for 12 hours; and (c) cooling the reaction kettle to room temperature after the reaction is completed, stirring the obtained black product with ethanol, centrifuging, and drying at 60 degrees C for 12 hours to obtain the target product.