• 专利标题:   Hydrothermal method loading graphene quantum dots on graphite paper, comprises e.g. heat-treating citric acid, submerging graphite paper in pretreatment solution, placing in polytetrafluoroethylene container for hydrothermal treatment and immersing in graphene quantum dot solution, and washing.
  • 专利号:   CN115472443-A
  • 发明人:   WANG Z, ZHAO Z, HU Y
  • 专利权人:   UNIV ZHEJIANG SCITECH
  • 国际专利分类:   H01G011/32, H01G011/86
  • 专利详细信息:   CN115472443-A 13 Dec 2022 H01G-011/86 202307 Chinese
  • 申请详细信息:   CN115472443-A CN10993268 18 Aug 2022
  • 优先权号:   CN10993268

▎ 摘  要

NOVELTY - Hydrothermal method loading graphene quantum dots on graphite paper, comprises (1) heat-treating citric acid at 150-210℃ for 15-45 minutes, when the solution turns from transparent to orange, regulating system pH is neutral and obtaining graphene quantum dot solution, (2) preparing a pretreatment solution with a concentration of 20-50 mM, submerging the graphite paper in the pretreatment solution and placing in a polytetrafluoroethylene container for hydrothermal treatment at 150-180℃ for 60-120 minutes, washing, and drying to obtain pre-treated graphite paper, and (3) immersing the graphite paper in the graphene quantum dot solution, and placing in a hydrothermal kettle for hydrothermal treatment at 100-180℃ for 60-180 minutes, washing with water and ethanol to remove unreacted residual solution to obtain graphite paper loaded with graphene quantum dots. USE - The method for loading quantum graphene on graphite paper by hydrothermal method and application thereof in preparation of plane micro-supercapacitor used in micro, portable electronic device e.g. human-computer interaction system, implantable medical monitoring module and extreme environment emergency energy. ADVANTAGE - The method realizes the integration of planar micro energy storage devices, and the all-round improvement of miniaturization, functionalization and electrochemical performance is of great significance to the scalable development and production of flexible and wearable electronic devices. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing micro super capacitor by laser cutting graphite paper loaded graphene quantum dots.