• 专利标题:   Preparing graphene involves e.g. mixing cooled concentrated sulfuric acid with graphite, sodium nitrate, potassium permanganate and hydrogen peroxide, reacting and washing with dilute hydrochloric acid.
  • 专利号:   CN110862079-A
  • 发明人:   ZHI T
  • 专利权人:   ZHI T
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN110862079-A 06 Mar 2020 C01B-032/184 202026 Pages: 3 Chinese
  • 申请详细信息:   CN110862079-A CN10986496 28 Aug 2018
  • 优先权号:   CN10986496

▎ 摘  要

NOVELTY - Preparing graphene, comprises (i) adding 115 ml concentrated sulfuric acid into 4-necked flask under mechanical stirring and ice bath condition, cooling to 4-5 degrees C, adding 5 g 400 mesh size graphite and 2.5 g sodium nitrate, stirring for 15 minutes, then slowly adding 35 g potassium permanganate, maintaining the temperature, and stirring at below 10 degrees C for 30 minutes, (ii) heating, and reacting at 35 degrees C for 60 minutes, (iii) adding 230 ml deionized water dropwise into the above mixture, heating at 95-98 degrees C, and stirring for 30 minutes, (iv) pouring the obtained product into 1 l deionized water, then adding hydrogen peroxide, and stirring until the product becomes yellow, and (v) washing the obtained product using 5% dilute hydrochloric acid and deionized water, respectively until the pH is 5. USE - The method is useful for preparing graphene. ADVANTAGE - The method has simple operation with easily controllable temperature.