• 专利标题:   Preparation of graphene oxide reinforced polylactic acid comprises washing graphite, drying, dissolving in deionized water, carrying out ultrasonic oscillation and high-vacuum melt polycondensation, decompressing, cooling and washing.
  • 专利号:   CN103086367-A
  • 发明人:   SHAN M, QIAN X, YANG C, YUE M, LI W, XU Z, GUO Q, MAI W
  • 专利权人:   UNIV TIANJIN POLYTECHNIC
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103086367-A 08 May 2013 C01B-031/04 201373 Pages: 6 Chinese
  • 申请详细信息:   CN103086367-A CN10014735 16 Jan 2013
  • 优先权号:   CN10014735

▎ 摘  要

NOVELTY - A graphene oxide reinforced polylactic acid is prepared by washing graphite, drying, dissolving in deionized water, carrying out ultrasonic oscillation to peel off graphite oxide, drying, adding lactic acid, placing in oil bath, decompressing, distilling, mixing anhydrous lactic acid and graphene oxide at mass ratio of 20:1-320:1, raising temperature to 160-190 degrees C, adding catalyst, carrying out high-vacuum melt polycondensation at not greater than 100 Pa, cooling, dissolving in chloroform and washing. USE - Method for preparing graphene oxide reinforced polylactic acid (claimed). ADVANTAGE - The method has simple process and low cost.