• 专利标题:   Continuous large-scale preparation of graphene comprises mixing graphite intercalation agent with supercritical fluid, stewing, mixing with graphite to obtain graphene suspension, homogenizing in high pressure homogenizer and filtering.
  • 专利号:   CN106185886-A
  • 发明人:   CHEN Q, ZENG J
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN106185886-A 07 Dec 2016 C01B-031/04 201709 Pages: 6 Chinese
  • 申请详细信息:   CN106185886-A CN10507575 01 Jul 2016
  • 优先权号:   CN10507575

▎ 摘  要

NOVELTY - Continuous large-scale preparation of graphene comprises (a) mixing graphite intercalation agent with supercritical fluid, stewing for 1-5 hours to obtain pre-intercalated layer mixed solution, (b) mixing with graphite to obtain graphene suspension, (c) taking the graphite suspension into a high pressure homogenizer for stripping and homogenizing and (d) filtering the high-pressure homogenizer liquid to obtain graphene, where the high pressure homogenizer having a homogenizing cavity inlet is provided with an ultrasonic wave generating source. USE - The method is useful for continuous large-scale preparation of graphene (claimed). ADVANTAGE - The method: improves the yield of grapheme; and has low production cost. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene powder, prepared by the above preparation method.