• 专利标题:   Three-dimensional porous nitrogen-doped graphene composite material preparation involves dissolving iron nitrate and polyvinylpyrrolidone in deionized water under to form mixed solution.
  • 专利号:   CN108264037-A
  • 发明人:   LI P, HAN K, LIU Z, WANG W, ZHAO W, AN F, QU X
  • 专利权人:   UNIV BEIJING SCI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, C01B032/184, C01B032/914
  • 专利详细信息:   CN108264037-A 10 Jul 2018 C01B-032/184 201860 Pages: 9 Chinese
  • 申请详细信息:   CN108264037-A CN10116559 06 Feb 2018
  • 优先权号:   CN10116559

▎ 摘  要

NOVELTY - Three-dimensional porous nitrogen-doped graphene composite material preparation involves dissolving iron nitrate and polyvinylpyrrolidone in deionized water under ultrasonic stirring for 3-15 minutes to form a mixed solution. The ferric nitrate and the polyvinylpyrrolidone are provided in a mass ratio of 1.0-3.0:1. The mixed solution is placed in a forced air oven for drying completely, and then ground into a powder, which is transferred to a crucible in a tube furnace at 500-900 degrees C in an inert protective atmosphere for 1-3 hours. The tube furnace is cooled at room temperature to give black foamy product. The obtained black foamy product is collected to give the three-dimensional porous nitrogen-doped graphene composite material. USE - Method for preparing three-dimensional porous nitrogen-doped graphene composite material. ADVANTAGE - The method prepares the three-dimensional porous nitrogen-doped graphene composite material in a simple, precise, cost-effective and eco-friendly manner with strong repeatability, large-scale preparation and broad application prospects in energy storage and catalysis fields. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic X-ray diffraction pattern of the three-dimensional porous nitrogen-doped graphene composite material modified by an iron carbide nanoparticle.