• 专利标题:   Preparing platinum-based alloy catalyst comprises dissolving cobalt salt in solvent, adding alkali containing ammonia to form sol, heating sol and mixing with carbon carrier, drying to remove solvent to obtain cobalt oxide modified carbon, and taking polyol as solvent.
  • 专利号:   CN114784294-A
  • 发明人:   ZHANG Y, LI J, DUAN X, WANG Y, LI X, LIU J
  • 专利权人:   CHINA AUTOMOTIVE INNOVATION CORP TECHNOL, UNIV NORTH CHINA ELECTRIC POWER
  • 国际专利分类:   H01M004/88, H01M004/92
  • 专利详细信息:   CN114784294-A 22 Jul 2022 H01M-004/88 202200 Chinese
  • 申请详细信息:   CN114784294-A CN11567153 20 Dec 2021
  • 优先权号:   CN11567153

▎ 摘  要

NOVELTY - Preparing platinum-based alloy catalyst comprises (i) dissolving a cobalt salt in a solvent, and adding alkali containing ammonia to form sol, (ii) heating the sol and mixing with carbon carrier, and drying to remove the solvent to obtain cobalt oxide modified carbon, and (iii) taking the carbon modified by a cobalt oxide as carrier, mixing with a platinum salt, taking polyol as the solvent, heating, adding acid to settle, removing the solvent, and washing to obtain platinum-based alloy catalyst. USE - The method for preparing platinum-based alloy catalyst useful in preparing proton exchange membrane fuel cell (claimed). ADVANTAGE - The method enables efficient and stable preparation of platinum-based alloy catalyst with high yield. The catalyst has stable property and has batch advantage. The reduction process can protect the reduced platinum nanoparticles by using the method of polyol reduction, avoiding particle aggregation. The method avoids the problem of difficult alloying caused by the difference of reduction potential, and avoids the long-time heating and reducing. The ammonium root buffer ions introduced in the process, can buffer the pH change of the reaction system. DETAILED DESCRIPTION - AN INDEPENDENT CLAIMS is also included for a platinum-based alloy catalyst, obtained by the method as mentioned.