• 专利标题:   Preparation of lithium titanate composite electrode material used as cathode material for e.g. power lithium-ion battery, involves mixing powdered graphene with polyethylene glycol, and adding polyethylene glycol solvent.
  • 专利号:   CN107579216-A
  • 发明人:   CHEN S, HAN J, HAN Y, MI X, RONG C, WANG D, ZHANG K, ZHANG Y
  • 专利权人:   CHINA FAW CO LTD
  • 国际专利分类:   H01G011/24, H01G011/46, H01M010/0525, H01M004/36, H01M004/485, H01M004/62
  • 专利详细信息:   CN107579216-A 12 Jan 2018 H01M-004/36 201810 Pages: 7 Chinese
  • 申请详细信息:   CN107579216-A CN10707470 17 Aug 2017
  • 优先权号:   CN10707470

▎ 摘  要

NOVELTY - The preparation method of lithium titanate composite electrode material involves (i) mixing powdered graphene with polyethylene glycol, adding 20-50 times polyethylene glycol solvent, ultrasonically dispersing in a solvent for 0.5-5 hours, specifically 2 hours to obtain a conductive graphene dispersion, (ii) mixing lithium titanate material and conductive graphene dispersion, ball milling in a planetary ball mill, (iii) drying the milled material, placing in an atmosphere furnace, sintering in an anaerobic inert gas, and grinding. USE - Preparation of lithium titanate composite electrode material used as cathode material for power lithium-ion battery and hybrid supercapacitor. ADVANTAGE - The method enables the preparation of lithium titanate composite electrode material with high electronic conductivity, and excellent rate performance. DETAILED DESCRIPTION - The preparation method of lithium titanate composite electrode material involves (i) mixing powdered graphene with polyethylene glycol in a ratio of 1:0.8-2, specifically 1:1, adding 20-50 times polyethylene glycol solvent, ultrasonically dispersing in a solvent for 0.5-5 hours, specifically 2 hours to obtain a conductive graphene dispersion, (ii) mixing lithium titanate material and conductive graphene dispersion in a ratio of 1:1-5, ball milling in a planetary ball mill for 2-10 hours, specifically 4 hours, (iii) drying the milled material, placing in an atmosphere furnace, sintering in an anaerobic inert gas at 500-800 degrees C, specifically 650 degrees C for 1-5 hours, specifically 2 hours, and grinding.