• 专利标题:   Preparation of graphene-titania fiber used for wastewater treatment, comprises ultrasonically dispersing graphene and tetrahydrofuran, adding ethyl acetoacetate and tetrabutyl titanate, heating, carrying out rotary evaporation and cooling.
  • 专利号:   CN103111274-A, CN103111274-B
  • 发明人:   GUAN J, ZHANG Q, HE S, ZHANG C, WU G, BAO N
  • 专利权人:   UNIV SHANDONG
  • 国际专利分类:   B01J021/18, B01J035/06
  • 专利详细信息:   CN103111274-A 22 May 2013 B01J-021/18 201370 Pages: 4 Chinese
  • 申请详细信息:   CN103111274-A CN10064816 28 Feb 2013
  • 优先权号:   CN10064816

▎ 摘  要

NOVELTY - Preparation of graphene-titania fiber comprises ultrasonically dispersing 0.15-0.20 g graphene and tetrahydrofuran, adding ethyl acetoacetate as chelating agent and tetrabutyl titanate, mixing, heating at 82 degrees C to reflux for 1 hour, adding deionized water, stirring, heating at 70 degrees C to reflux for 1 hour, carrying out rotary evaporation until viscosity is 5-75 Pa-second, maintaining temperature at 25-450 degrees C under nitrogen atmosphere, and cooling. USE - Method for preparing graphene-titania fiber (claimed) used for wastewater treatment. ADVANTAGE - The fiber has excellent photocatalytic property.