• 专利标题:   Preparation of graphene-nanosilver dispersion liquid involves mixing graphite powder and dispersant with solvent, adding polyvinylpyrrolidone aqueous solution, graphene solution, silver nitrate solution and reducing agent, and stirring.
  • 专利号:   CN106903324-A
  • 发明人:   LIU P, NING T, NING W, HU W
  • 专利权人:   HUNAN LEED THICK FILM PASTE CO LTD
  • 国际专利分类:   B22F009/24, B82Y040/00, C01B032/184
  • 专利详细信息:   CN106903324-A 30 Jun 2017 B22F-009/24 201758 Pages: 4 Chinese
  • 申请详细信息:   CN106903324-A CN10970957 22 Dec 2015
  • 优先权号:   CN10970957

▎ 摘  要

NOVELTY - The preparation method of graphene-nanosilver dispersion liquid involves adding graphite powder and dispersant to solvent and then uniformly mixing, heating the mixture at 90-110 degrees C for 0.5-2 hours and then centrifugally separating at 4000 rpm, adding polyvinylpyrrolidone aqueous solution, graphene solution and silver nitrate solution to the mixture and then reacting for 1-10 minutes, uniformly stirring the mixture and then adjusting pH value, stirring the mixture for 0.5-1 hour and increasing temperature at 40-80 degrees C, adding reducing agent to the mixture, and stirring. USE - The method is useful for preparation of graphene-nanosilver dispersion liquid (claimed). ADVANTAGE - The method enables simple and easy preparation of graphene-nanosilver dispersion liquid with high efficiency and excellent electrical conductivity and dispersibility. DETAILED DESCRIPTION - The preparation method of graphene-nanosilver dispersion liquid involves adding graphite powder and dispersant to solvent and then uniformly mixing, heating the mixture at 90-110 degrees C for 0.5-2 hours and then centrifugally separating at 4000 rpm, adding polyvinylpyrrolidone aqueous solution, graphene solution and silver nitrate solution to the mixture and then reacting for 1-10 minutes under a power of 100-400 W, uniformly stirring the mixture and then adjusting pH value, ultrasonically stirring the mixture for 0.5-1 hour and then increasing temperature at 40-80 degrees C, adding reducing agent to the mixture, and ultrasonically stirring for 1.5-2 hours.