• 专利标题:   Production of cobalt-ferrite-graphene lithium ion battery by pretreating steel rolling oil sludge with petroleum ether, adding dilute sulfuric acid solution, stirring, centrifuging, concentrating, evaporating, standing, and crystallizing.
  • 专利号:   CN105895885-A, CN105895885-B
  • 发明人:   CHANG X, CHEN D, CHEN H, HAN S, LI Y, LIN H, LIU P, PEI S, XUE Y, WANG A, XU G, ZHOU J, ZHAO Z, HAN Z
  • 专利权人:   SHANGHAI INST TECHNOLOGY, SHANGHAI INST TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/52, H01M004/583
  • 专利详细信息:   CN105895885-A 24 Aug 2016 H01M-004/36 201670 Pages: 8 Chinese
  • 申请详细信息:   CN105895885-A CN10438479 17 Jun 2016
  • 优先权号:   CN10438479

▎ 摘  要

NOVELTY - Production of cobalt-ferrite-graphene lithium ion battery includes pretreating steel rolling oil sludge with petroleum ether, adding dilute sulfuric acid solution, water bath stirring, and centrifuging; concentrating, evaporating, standing, crystallizing, dissolving crystals in water, and oxidizing with hydrogen peroxide; adding cobalt nitrate hexahydrate and graphite, adjusting to alkaline using sodium hydroxide, heating, stirring to co-precipitate, washing, and vacuum-drying; and calcining, slicing, and encapsulating. USE - Method for production of cobalt-ferrite-graphene lithium ion battery (claimed). ADVANTAGE - The method fully utilizes waste steel rolling oil sludge. The battery has good performance. DETAILED DESCRIPTION - Production of cobalt-ferrite-graphene lithium ion battery comprises pretreating steel rolling oil sludge with petroleum ether, adding dilute sulfuric acid solution, water bath stirring, and centrifuging to separate unreacted non-ferrous solid residues and obtain ferrous sulfate solution; concentrating, evaporating, standing at - 10-5 degrees C, crystallizing, dissolving ferrous sulfate crystals in water, and oxidizing with hydrogen peroxide; adding cobalt nitrate hexahydrate and graphite, adjusting to alkaline using sodium hydroxide, heating, stirring to co-precipitate, washing, and vacuum-drying; and calcining to 300-600 degrees C under inert atmosphere to remove oxygen-containing groups, slicing, and encapsulating.