• 专利标题:   Preparing high quality and low cost vanadium nitride iron alloy comprises e.g. adding vanadium source compound, iron source compound and reducing agent into de-ionized water, stirring to obtain mixed solution, and adding citric acid.
  • 专利号:   CN112575239-A
  • 发明人:   ZHANG C
  • 专利权人:   HUNAN ZHONGXIN NEW MATERIAL TECHNOLOGY
  • 国际专利分类:   B22F009/24, C22C001/05, C22C027/02, C22C035/00
  • 专利详细信息:   CN112575239-A 30 Mar 2021 C22C-035/00 202134 Pages: 7 Chinese
  • 申请详细信息:   CN112575239-A CN11423550 08 Dec 2020
  • 优先权号:   CN11423550

▎ 摘  要

NOVELTY - Preparing high quality and low cost vanadium nitride iron alloy comprises (1) adding vanadium source compound, iron source compound, reducing agent into deionized water, and stirring to obtain mixed solution, (2) adding citric acid into obtained mixed solution, and performing ultrasonic stirring reaction for more than 4 hours to obtain uniform sol, (3) drying obtained sol to obtain dry gel, and grinding into powder to obtain solid powder, (4) and adding 0.06-0.08 wt.% graphene oxide into solid powder, roasting at 360-370 degrees C for more than 5 hours, and quenching to room temperature to obtain vanadium nitride iron alloy. USE - The method is useful for preparing high quality and low cost vanadium nitride iron alloy. ADVANTAGE - The method enables economical preparation of high-quality vanadium nitride iron alloy with vanadium content of 69.5-71 %, nitrogen content of 17.8-18 % and purity of more than 99.2%.