• 专利标题:   Preparation of organosilane oligomer-modified graphene, by reacting graphene oxide and dry anhydrous solvent, ultrasonically dispersing, adding chlorosilane and deionized water, filtering, concentrating filtrate, distilling and drying.
  • 专利号:   CN108002377-A
  • 发明人:   REN H, FAN Z, SUN Q, ZHANG P, LIU M
  • 专利权人:   AECC BEIJING AERONAUTICAL MATERIALS INST
  • 国际专利分类:   C01B032/194, C01B032/184
  • 专利详细信息:   CN108002377-A 08 May 2018 C01B-032/194 201845 Pages: 5 Chinese
  • 申请详细信息:   CN108002377-A CN11186739 23 Nov 2017
  • 优先权号:   CN11186739

▎ 摘  要

NOVELTY - Preparation of organosilane oligomer-modified graphene involves adding 10 pts. wt. graphene oxide prepared by oxidation-reduction method to three-port reaction bottle, adding dry anhydrous solvent, sealing bottle, reacting, ultrasonically dispersing mixed system for 40-90 minutes to obtain dispersion system, stirring, adding 5-100 pts. wt. chlorosilane, reacting for 24-48 hours to obtain chlorosilane-modified graphene, adding 0.5-15 pts. wt. deionized water and 10-100 pts. wt. tetrahydrofuran, reacting for 10-15 minutes to obtain organosilane oligomer-modified graphene dispersion, cooling to room temperature, filtering under vacuum conditions, washing filtrate with water, concentrating filtrate, distilling and drying. The thickness of graphene oxide is 0.5-10 nm. The anhydrous solvent comprises tetrahydrofuran, methyltetrahydrofuran or cyclohexane. USE - Preparation of organosilane oligomer-modified graphene.