• 专利标题:   Preparation of reduced graphene oxide loaded palladium-metal precursor nano composite catalyst involves preparing final mixed solution using e.g. graphene oxide, dripping sodium borohydride solution, vacuum-filtering and freeze-drying.
  • 专利号:   CN108155392-A
  • 发明人:   XU M, JI J, ZHANG Y, DONG P, CENG X, LI X, LIN Y, YANG X, HUO Q
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   H01M004/88, H01M004/92
  • 专利详细信息:   CN108155392-A 12 Jun 2018 H01M-004/92 201846 Pages: 16 Chinese
  • 申请详细信息:   CN108155392-A CN11233090 30 Nov 2017
  • 优先权号:   CN11233090

▎ 摘  要

NOVELTY - Preparation of reduced graphene oxide loaded palladium-metal precursor nano composite catalyst involves (S1) ultrasonically dispersing a graphene oxide in ultra-pure water to obtain a graphene oxide suspension with a concentration of 0.1-2 mg/mL, (S2) mixing a salt solution of sodium tetrachloropalladate solution and metal precursor in a molar ratio of 1:1-5:1, adding dispersion to the graphene oxide suspension, dispersing the metal precursor between the graphene oxide nanosheets, uniformly mixing with polyethylene glycol to obtain a final mixed solution, (S3) dripping 0.005-0.05 mol/L sodium borohydride solution to the final mixed solution, stirring and loading the mixture, washing using a mixture of deionized water and anhydrous ethanol, vacuum-filtering, and freeze-drying. The ratio between the volume of polyethylene glycol and the mass of graphene oxide is 1-3 mL/mg. USE - Preparation of reduced graphene oxide loaded palladium-metal precursor nano composite catalyst. ADVANTAGE - The process is simple and feasible, and produces catalyst having uniform Dispersibility, large specific surface area, improved catalytic activity and stability.