• 专利标题:   Preparation of high energy density graphene battery anode material involves mixing graphene oxide, absolute ethanol, silicate and iron salt solution, hydrolyzing, heat-preserving, cleaning with hydrofluoric acid, washing, and drying.
  • 专利号:   CN111129495-A
  • 发明人:   CHEN K
  • 专利权人:   CHEN K
  • 国际专利分类:   H01M010/0525, H01M004/587, H01M004/62
  • 专利详细信息:   CN111129495-A 08 May 2020 H01M-004/587 202044 Pages: 7 Chinese
  • 申请详细信息:   CN111129495-A CN11341198 23 Dec 2019
  • 优先权号:   CN11341198

▎ 摘  要

NOVELTY - Preparation of high energy density graphene battery anode material involves (1) mixing 10-30 pts. wt. graphene oxide, 80-120 pts. wt. absolute ethanol and 1-5 pts. wt. silicate, ultrasonically dispersing, obtaining dispersion, (2) dripping 1-10 pts. wt. iron salt solution into the dispersion, stirring, hydrolyzing, obtaining hydrolyzate, (3) spraying drying the hydrolyzate, obtaining precursor, (4) placing the precursor in a hydrogen atmosphere, heating to 800-1000 degrees C, heat-preserving, passing in organic alkane gas under the condition of 1000-1500 degrees C, performing high temperature reaction to reduce graphene, (6) ultrasonically cleaning the reduced graphene with hydrofluoric acid, washing, and drying. USE - Preparation of high energy density graphene battery anode material. ADVANTAGE - The preparation method provides graphene battery anode material having wide layer spacing, large specific surface area, and agglomeration resistance. The electrode material has large energy density and excellent cycle stability.