• 专利标题:   Preparing graphene/polybutylene succinate composite film involves lyophilizing polybutylene succinate and rapidly pulverizin, uniformly dispersing graphene in solvent to form mixed solution, pulverizing polybutylene succinate.
  • 专利号:   CN108659474-A
  • 发明人:   HUANG J, CUI C, YAN G
  • 专利权人:   UNIV NINGDE NORMAL
  • 国际专利分类:   C08L067/02, C08K003/04, C08J005/18, C09K005/14
  • 专利详细信息:   CN108659474-A 16 Oct 2018 C08L-067/02 201882 Pages: 8 Chinese
  • 申请详细信息:   CN108659474-A CN10297923 19 Aug 2016
  • 优先权号:   CN10297923, CN10688924

▎ 摘  要

NOVELTY - Preparing graphene/polybutylene succinate composite film involves lyophilizing polybutylene succinate and rapidly pulverizin, uniformly dispersing graphene in a solvent to form a mixed solution, pulverizing polybutylene succinate, adding to the mixed solution, stirring uniformly, covering graphene on the surface of the polybutylene succinate, drying the product, placing the product at 120 degrees C in a double roll. The coiler is subjected to a wrapping roller until a smooth and uniform surface is obtained, and then the sheet temperature is gradually lowered to 90 degrees C to obtain a graphene/polybutylene succinate composite film. The graphene/polybutylene succinate composite film has a lamellar structure and has a smooth shape surface structure, graphene/polybutylene succinate composite film includes a polybutylene succinate matrix and a graphene powder uniformly covering the surface of the polybutylene succinate substrate. USE - Method for preparing graphene/polybutylene succinate composite film. ADVANTAGE - The method enables to prepare graphene/polybutylene succinate composite film which has better elongation at break, and reduced the Young's modulus. DETAILED DESCRIPTION - Preparing graphene/polybutylene succinate composite film involves lyophilizing polybutylene succinate and rapidly pulverizin, uniformly dispersing graphene in a solvent to form a mixed solution, pulverizing polybutylene succinate, adding to the mixed solution, stirring uniformly, covering graphene on the surface of the polybutylene succinate, drying the product, placing the product at 120 degrees C in a double roll. The coiler is subjected to a wrapping roller until a smooth and uniform surface is obtained, and then the sheet temperature is gradually lowered to 90 degrees C to obtain a graphene/polybutylene succinate composite film. The graphene/polybutylene succinate composite film has a lamellar structure and has a smooth shape surface structure, graphene/polybutylene succinate composite film includes a polybutylene succinate matrix and a graphene powder uniformly covering the surface of the polybutylene succinate substrate, and the graphene/polybutylene succinate composite film has mass content of graphene is 0.1%, 0.5%, 0.7% or 0.9%.