• 专利标题:   Synthesis of fluorinated graphene oxide used for detection of heavy metal ion, involves mixing graphite with acid solution, adding potassium permanganate to mixture, adding mixture to container containing ice, separating solid, and rinsing.
  • 专利号:   CA2991734-A1, US2018251378-A1
  • 发明人:   CHEN A
  • 专利权人:   UNIV LAKEHEAD, UNIV LAKEHEAD
  • 国际专利分类:   C01B032/198, C01B032/182, G01N027/416, G01N027/48, G01N027/30, C07D301/00
  • 专利详细信息:   CA2991734-A1 13 Jul 2018 C01B-032/198 201857 Pages: 20 English
  • 申请详细信息:   CA2991734-A1 CA2991734 12 Jan 2018
  • 优先权号:   US446114P, US508080P, US869785

▎ 摘  要

NOVELTY - Synthesis of 0.5-1.5 atomic% fluorinated graphene oxide (FGO) involves, mixing n grams of graphite with solution of 5x n-40x n ml hydrofluoric acid and 50x n-150x n ml sulfuric acid or phosphoric acid with stirring at 30-80 degrees C for time (t1), adding 3x n-10x n g potassium permanganate to mixture and stirring the mixture at 40-80 degrees C for time (t2), adding reacted mixture to container containing 50x n-250x n ml ice and hydrogen peroxide, separating solid comprising 0.5-1.5 atomic% FGO from mixture, rinsing and drying the FGO. USE - Synthesis of fluorinated graphene oxide used for detection of heavy metal ions such as cadmium, lead, cupric, and mercury, and improvement in electrochemical sensing application. Can also be used for battery, biomedical device, capacitors, catalyst support and sensor. ADVANTAGE - The process provides FGO with improved electrochemical and structural properties. The heavy metal ion stripping is performed efficiently using metal-free FGO.