• 专利标题:   Preparing graphene oxide composite material involves preparing graphene oxide solution, preparing four-arm poly(ethylene glycol)-polycaprolactone-poly(ethylene glycol) solution, and mixing graphene oxide solution.
  • 专利号:   CN106832844-A, CN106832844-B
  • 发明人:   LIN Y, HUANG Q, CAI X, GONG T, HAO L
  • 专利权人:   UNIV SICHUAN, UNIV SICHUAN
  • 国际专利分类:   C08J003/24, C08J003/28, C08K003/04, C08K009/00, C08L067/06
  • 专利详细信息:   CN106832844-A 13 Jun 2017 C08L-067/06 201759 Pages: 10 Chinese
  • 申请详细信息:   CN106832844-A CN10072901 10 Feb 2017
  • 优先权号:   CN10072901

▎ 摘  要

NOVELTY - Preparing graphene oxide composite material involves preparing graphene oxide solution, preparing four-arm poly(ethylene glycol)-polycaprolactone-poly(ethylene glycol) solution, mixing graphene oxide solution with four-arm poly(ethylene glycol)-polycaprolactone-poly(ethylene glycol) solution so that concentration of the graphene oxide in mixed solution is 0.15-0.4 wt.%, and adding mixture volume of 8-12 wt.% of photoinitiator, and mixing uniformly to obtain solid. USE - Method for preparing graphene oxide composite material (claimed). ADVANTAGE - The method enables to prepare graphene oxide composite material which has greatly improved strength and biocompatibility. DETAILED DESCRIPTION - Preparing graphene oxide composite material involves preparing graphene oxide solution, preparing four-arm poly(ethylene glycol)-polycaprolactone-poly(ethylene glycol) solution, mixing graphene oxide solution with four-arm poly(ethylene glycol)-polycaprolactone-poly(ethylene glycol) solution so that concentration of the graphene oxide in mixed solution is 0.15-0.4 wt.%, and adding mixture volume of 8-12 wt.% of photoinitiator, and mixing uniformly to obtain solid. The solid is melted at 60 degrees C, mixture is homogeneously stirred, placed in uniform film, and placed in a UV cross-linking apparatus at light intensity of 390-410 uw/square centimeter for 25-35 minutes, cooling material, and stripping down composite material to obtain final product.