• 专利标题:   Preparing rice hull-based graphene porous carbon material for preparing electrode, involves mixing nickel element and rice hull, immersing rice hull in nickel salt solution, stirring, drying, and carbonizing rice hull-nickel salt mixture.
  • 专利号:   CN109019567-A
  • 发明人:   JIN H, BAI Y, WU S, XU H, ZHANG Y, LI T, YE L, CHEN R, WANG Y
  • 专利权人:   UNIV XIAN JIAOTONG SUZHOU ACAD
  • 国际专利分类:   C01B032/184, H01G011/32, H01G011/26, H01G011/86
  • 专利详细信息:   CN109019567-A 18 Dec 2018 C01B-032/184 201919 Pages: 11 Chinese
  • 申请详细信息:   CN109019567-A CN11124325 26 Sep 2018
  • 优先权号:   CN11124325

▎ 摘  要

NOVELTY - The method for preparing rice hull-based graphene porous carbon material involves mixing nickel element and rice hull in ratio of 0.03-0.06:1, immersing rice hull in the nickel salt solution, stirring and drying to obtain rice hull-nickel salt mixture, carbonizing rice hull-nickel salt mixture at 700 degrees C to obtain RHNi-700, removing nickel salt particles in the RHNi-700, acid soaking, washed and drying to obtain RHNi-700A, dissolving RHNi-700A and alkali in water in mass ratio of 1:3-5, uniformly mixing and drying, heating under an inert gas atmosphere, drying and activating. USE - The method is useful for preparing rice hull-based graphene porous carbon material for preparing electrode (all claimed). ADVANTAGE - The method enables simple and economical preparation of rice hull-based graphene porous carbon material with high volume specific capacity and specific capacitance. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) rice hull-based graphene porous carbon material prepared by the method; (2) electrode, which comprises rice hull-based graphene porous carbon material, conductive carbon black, PTFE and nickel foam; and (3) preparation method of electrode, which involves mixing rice hull-based graphene porous carbon material, conductive carbon black and PTFE with an anhydrous ethanol solution in mass ratio of 8:1:1, coating obtained slurry on the substrate, placing foamed nickel in the coated slurry, and drying at 80 degrees C for 12 hours.