• 专利标题:   Preparation of reduced graphene oxide film, involves ultrasonically processing graphite oxide dispersion liquid, stirring, taking upper liquid, filtering, dissolving agar, mixing with prepared solution, cooling, and pasting adhesive tape.
  • 专利号:   CN108383109-A
  • 发明人:   ZHANG T, LIU Q, LIU J, YU J, CHEN R, CAO D, ZHANG H, XING T
  • 专利权人:   UNIV HARBIN ENGINEERING, HARBIN HAINENGTUO TECHNOLOGY DEV CO LTD
  • 国际专利分类:   C01B032/184, C08J005/18, C08K003/04, C08L005/12
  • 专利详细信息:   CN108383109-A 10 Aug 2018 C01B-032/184 201865 Pages: 5 Chinese
  • 申请详细信息:   CN108383109-A CN10334091 14 Apr 2018
  • 优先权号:   CN10334091

▎ 摘  要

NOVELTY - The preparation method of reduced graphene oxide film involves (1) using graphite oxide dispersion liquid, placing in an ultrasonic machine, ultrasonically processing for 2-5 hours, uniformly stirring using a centrifuge, taking upper liquid, and filtering the sediment to prepare graphene oxide solution with specified concentration, (2) dissolving a certain amount of agar under the condition of 300-400 K water bath, and magnetically stirring for 1 hour to form uniform agar aqueous solution, (3) mixing prepared graphene oxide solution and agar aqueous solution, and magnetically stirring for 4-10 hours to obtain a homogeneous solution under the condition of 300-400 K, (4) cooling the solution to room temperature, scraping on PTFE-lined scraper blade, pasting corresponding adhesive tape according to the required thickness, and drying to obtain graphene oxide film, and (5) calcining the graphene oxide thin film in a tubular furnace under nitrogen atmosphere. USE - Preparation method of reduced graphene oxide film. ADVANTAGE - The method enables preparation of reduced graphene oxide film with uniform and stable film-forming effect, even and controllable thickness, by simple and economical process.