• 专利标题:   Preparing gold nanorod/graphene oxide composite material involves grinding graphene oxide and mixing sodium polystyrene sulfonate polymer solution and subjected to ultrasonic reaction and then centrifuged to obtain clean liquid.
  • 专利号:   CN105750558-A, CN105750558-B
  • 发明人:   CHEN B, YAO A, ZHU H, SUN B
  • 专利权人:   UNIV TONGJI
  • 国际专利分类:   B22F001/02, B22F009/22, B82Y030/00, B82Y040/00
  • 专利详细信息:   CN105750558-A 13 Jul 2016 B22F-009/22 201673 Pages: 8 Chinese
  • 申请详细信息:   CN105750558-A CN10222312 12 Apr 2016
  • 优先权号:   CN10222312

▎ 摘  要

NOVELTY - Preparing gold nanorod/graphene oxide composite material involves weighing proper amount of graphene oxide and carrying out grinding. The 0.1-2mg obtained graphene oxide and 0.1g sodium polystyrene sulfonate polymer solution are mixed and subjected to ultrasonic reaction with power of 500-1000W for 30 minutes, and then centrifuged to obtain clean liquid. The obtained clean liquid is re-dispersed in proper amount of water. USE - Method for preparing gold nanorod/graphene oxide composite material (claimed). ADVANTAGE - The method enables to prepare gold nanorod/graphene oxide composite material, which has mild reaction condition, simple operation, short time, strong repeatability, implements diagnosis and treatment efficiency and has wide prospect for embellished antibody and loaded-drug. DETAILED DESCRIPTION - Preparing gold nanorod/graphene oxide composite material involves weighing proper amount of graphene oxide and carrying out grinding. The 0.1-2mg obtained graphene oxide and 0.1g sodium polystyrene sulfonate polymer solution are mixed and subjected to ultrasonic reaction with power of 500-1000W for 30 minutes, and then centrifuged to obtain clean liquid. The obtained clean liquid is re-dispersed in proper amount of water. The 5mL of 2M hexadecyltrimethylammonium bromide solution, 625 mu L of 0.008M chloroauric acid solution, 3.975mL deionized water, graphene oxide solution product, 300 mu L of 0.004M silver nitrate, 12 mu L concentrated hydrochloric acid, 75 mu Lof 85.8mM ascorbic acid, and 7.5 mu L of 0.01M sodiumm borohydride solution are mixed for 30 seconds, and shaken at 25-30 degrees C for 4-24 hours to obtain shaken material. The obtained shaken material is subjected to centrifugation at speed of 14000 revolutions per minute for 20 minutes. The pellet is re-dispersed in water to obtain final product.