• 专利标题:   Preparing sulfur-doped lithium titanate/graphene oxide composite material for sodium ion battery, by preparing titanium source solution and lithium salt solution, mixing, adding and graphene oxide, sintering and mixing with sulfur source.
  • 专利号:   CN110620221-A
  • 发明人:   REN Y, LIANG K
  • 专利权人:   UNIV CHANGZHOU
  • 国际专利分类:   H01M010/054, H01M004/36, H01M004/38, H01M004/485, H01M004/583
  • 专利详细信息:   CN110620221-A 27 Dec 2019 H01M-004/36 202004 Pages: 10 Chinese
  • 申请详细信息:   CN110620221-A CN10837379 05 Sep 2019
  • 优先权号:   CN10837379

▎ 摘  要

NOVELTY - Method for preparing a sulfur-doped lithium titanate/graphene oxide composite material, involves (a) dissolving a titanium source in a solution and stirring to obtain a titanium source solution, (b) dissolving a lithium source in deionized water and stirring to obtain a lithium salt solution, (c) adding the lithium salt solution to the titanium source solution and stirring to obtain a mixed solution, (d) adding polyvinylpyrrolidone (PVP), and graphene oxide to the mixed solution, ultrasonically dispersing, performing a hydrothermal reaction, and centrifuging and drying to obtain a lithium titanate/graphene oxide precursor, (e) sintering the precursor in a reducing atmosphere to obtain a lithium titanate/graphene oxide composite material, and mixing the composite material with a sulfur source and sintering in a reducing atmosphere to obtain a sulfur doped lithium titanate/graphene oxide composite material. USE - The method is useful for preparing a sulfur-doped lithium titanate/graphene oxide composite material, which is used as an active material for a negative electrode of a sodium ion battery (all claimed). ADVANTAGE - The sodium ion battery prepared using the composite material has high capacity.