• 专利标题:   Preparation of D-pi-A organic molecule-based structure graphene composite gas-sensing material involves dispersing graphene oxide in d water, sonicating, heating with organic molecule and hydrazine hydrate, and dispersing in water.
  • 专利号:   CN106082181-A, CN106082181-B
  • 发明人:   WANG Y, PEI W
  • 专利权人:   UNIV BEIHANG, UNIV BEIHANG
  • 国际专利分类:   C01B031/04, G01N027/12, C01B032/184
  • 专利详细信息:   CN106082181-A 09 Nov 2016 C01B-031/04 201709 Pages: 11 Chinese
  • 申请详细信息:   CN106082181-A CN10392820 06 Jun 2016
  • 优先权号:   CN10392820

▎ 摘  要

NOVELTY - Preparation of D-pi-A organic molecule-based structure graphene composite gas-sensing material comprises weighing graphene oxide, dispersing in deionized water to prepare 1 mg/mL dispersion, and sonicating for 40 minutes and 1 hour; adding organic molecule having D-pi-A structure, mixing, sonicating, where ratio of organic molecules to matrix material is 20:1; adding hydrazine hydrate, oil bath heating at 80 degrees C for 1 hour, and reduction reacting, where mass ratio of hydrazine hydrate and graphene oxide is 3:1; and vacuum filtering, repeatedly washing, and dispersing in deionized water. USE - Method for preparing D-pi-A organic molecule-based structure graphene composite gas-sensing material (claimed). ADVANTAGE - The material high selectivity and sensitivity, good recovery and stability, and low cost and is environment-friendly. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for gas-sensitive detection comprising take 0.1 mL dispersion, adding to test electrodes, heating at 40 degrees C, and drying; connecting to gas sensing equipment; testing 1-2 ppm nitrogen dioxide; testing gas with 10 ppm ammonia, methanol, acetone, and ethanol; and placing at different times and testing nitrogen dioxide.