• 专利标题:   Preparation of graphene doped lithium iron phosphate by mixing lithium source, iron salt, phosphorus salt, graphene and/or doped metal element, ball milling, calcining, adding carbon source, grinding, vacuum drying, firing, and crushing.
  • 专利号:   CN103579617-A
  • 发明人:   CHENG D, MA M, XU Y, YIN Z, WANG M
  • 专利权人:   HENAN KELONG GROUP CO LTD
  • 国际专利分类:   C01B025/45, H01M004/58, H01M004/62
  • 专利详细信息:   CN103579617-A 12 Feb 2014 H01M-004/58 201426 Pages: 8 Chinese
  • 申请详细信息:   CN103579617-A CN10254830 20 Jul 2012
  • 优先权号:   CN10254830

▎ 摘  要

NOVELTY - A graphene doped lithium iron phosphate is prepared by mixing lithium source compound, iron salt compound, phosphorus salt, and graphene or doped metal element at molar ratio of 0.95-1.05:1:1:0.05-0.5, ball milling at less than or equal to 40 degrees C for 3-10 hours, calcining at 350-500 degrees C for 7-15 hours in nitrogen or argon gas, adding carbon source at mass ratio of 1:0.02-0.1, grinding in ball mill with dispersant at less than or equal to 40 degrees C for 3-10 hours, vacuum drying, firing at 650-800 degrees C for 7-15 hours in nitrogen or argon gas, crushing, and classifying. USE - Method for preparing graphene doped lithium iron phosphate (claimed). ADVANTAGE - The preparation improves the conductivity, ion diffusion rate, and performance of the material.