• 专利标题:   Preparing graphene/ZIF-7 composite gel comprises preparing graphene gel by ultrasonically dispersing graphene oxide solid powder in distilled water, dissolving L-ascorbic acid and reacting to form columnar graphene gel, exchanging the solvent with dimethylformamide and immersing the graphene gel.
  • 专利号:   CN115608281-A
  • 发明人:   LI C, HE N, QIAO Y
  • 专利权人:   UNIV LANZHOU JIAOTONG
  • 国际专利分类:   B01J013/00, C01B032/19
  • 专利详细信息:   CN115608281-A 17 Jan 2023 B01J-013/00 202317 Chinese
  • 申请详细信息:   CN115608281-A CN10789636 13 Jul 2021
  • 优先权号:   CN10789636

▎ 摘  要

NOVELTY - Preparing graphene/ZIF-7 composite gel comprises regulating the concentration of zinc nitrate hexahydrate and benzimidazole, the composite gel with controllable ZIF-7 load capacity is prepared, and consists of the following steps: (a) preparing graphene gel by ultrasonically dispersing graphene oxide solid powder in distilled water, dissolving L-ascorbic acid and reacting at 95°C for 2 hours to form columnar graphene gel, (b) exchanging the solvent with dimethylformamide (DMF), immersing the graphene gel prepared in step (a) in the DMF solution of zinc nitrate hexahydrate, and allowing to stand for 24 hours, washing with DMF 3 times, immersing in the DMF solution of benzimidazole, and allowing to stand for 24 hours to obtain graphene /ZIF-7 composite gel (GO/ZIF-7). USE - The method is useful for preparing graphene/ZIF-7 composite gel. ADVANTAGE - The graphene/ZIF-7 composite gel is suitable for water purification, gas separation and storage field.