• 专利标题:   Method for preparing molybdenum disulfide/graphene nano-composite material used in lithium-sulfur battery, involves dispersing graphene oxide, and adding sodium thiomolybdate and elemental sulfur followed by refluxing, separating and drying.
  • 专利号:   CN104051735-A, CN104051735-B
  • 发明人:   LI Y, ZHANG F, WANG S, WANG Z, BI S, XIA J, XIA L, XIA Y
  • 专利权人:   UNIV QINGDAO
  • 国际专利分类:   H01M004/58, H01M004/62
  • 专利详细信息:   CN104051735-A 17 Sep 2014 H01M-004/58 201481 Pages: 6 Chinese
  • 申请详细信息:   CN104051735-A CN10301364 27 Jun 2014
  • 优先权号:   CN10301364

▎ 摘  要

NOVELTY - A molybdenum disulfide/graphene nano-composite material preparing method involves dispersing graphene oxide in deionized water to graphene oxide water solution. The obtained graphene oxide water solution is added with sodium thiomolybdate and elemental sulfur at 95 degrees C and allowed for reflux process to obtain solid product followed by separating using centrifugation, washing using deionized water and vacuum drying at 100-800 degrees C for 3-5 hours to obtain the finished product. USE - Method for preparing a molybdenum disulfide/graphene nano-composite material used in a lithium-sulfur battery (claimed). ADVANTAGE - The method enables preparing the composite material with porous spherical structure and increased lithium-sulfur battery property in a simple and cost-effective manner. DETAILED DESCRIPTION - A molybdenum disulfide/graphene nano-composite material preparing method involves dispersing graphene oxide in deionized water to graphene oxide water solution. The obtained graphene oxide water solution is added with sodium thiomolybdate and elemental sulfur at 95 degrees C and allowed for reflux process to obtain solid product followed by separating using centrifugation, washing using deionized water and vacuum drying at 100-800 degrees C for 3-5 hours to obtain the finished product, where the mass ratio of graphene oxide and deionized water is 1:300, the mass ratio of graphene oxide and sodium thiomolybdate is 1:2-4 and the mass ratio of graphene oxide and elemental sulfur is 1:6-10.