• 专利标题:   Synthesizing corundum nanoparticles by mixing reaction precursor with conductive additive to form mixture, where precursor is aluminum compound and applying voltage across mixture for nanoparticles, where voltage is applied in voltage pulses and voltage pulses increase temperature of mixture.
  • 专利号:   WO2022067102-A1, WO2022067102-A9
  • 发明人:   TOUR J M, DENG B
  • 专利权人:   UNIV RICE WILLIAM MARSH
  • 国际专利分类:   B09B003/00, C01B032/914, C01B032/921, C01B032/949, C01B032/956, C01B032/991, C01F007/02, C04B035/10, C22B011/00
  • 专利详细信息:   WO2022067102-A1 31 Mar 2022 202240 Pages: 213 English
  • 申请详细信息:   WO2022067102-A1 WOUS052057 24 Sep 2021
  • 优先权号:   US082592P

▎ 摘  要

NOVELTY - Method of synthesizing corundum nanoparticles involves mixing a reaction precursor with a conductive additive to form a mixture, where the reaction precursor is an aluminum compound; and applying a voltage across the mixture to form the corundum nanoparticles, where the voltage is applied in voltage pulses, duration of each of the voltage pulses is for a duration period, and the voltage pulses increase the temperature of the mixture to at most 1500 K. USE - The method is useful for synthesizing corundum nanoparticles. ADVANTAGE - The method meets the need for a rapid and energy-efficient pretreatment for the REE recovery from ores, fly ash, and bauxite residue (red mud) and the need to develop a 'dry' method to directly recovery the rare earth elements in ores, fly ash, and bauxite residue (red mud). DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a system for performing the above method comprising (a) a source of the mixture comprising the material and conductive additive; (b) a cell operably connected to the source such that the mixture can be flowed into the cell and held under compression; (c) electrodes operatively connected to the cell; and (d) a flash power supply for applying a voltage across the mixture to recover the metal from the material.