• 专利标题:   Low-temperature preparation of alpha-phase aluminum oxide powder for e.g. refractory flame-retardant material, involves using calcining additive chosen from carbon black, graphene, carbon nanotube and gas-phase growth carbon fiber.
  • 专利号:   CN116253346-A
  • 发明人:   LI T, YAN Z, CAO W
  • 专利权人:   YIBIN NANMU NANO TECHNOLOGY CO LTD
  • 国际专利分类:   C01F007/442
  • 专利详细信息:   CN116253346-A 13 Jun 2023 C01F-007/442 202355 Chinese
  • 申请详细信息:   CN116253346-A CN10279915 21 Mar 2023
  • 优先权号:   CN10279915

▎ 摘  要

NOVELTY - Low-temperature preparation of α-phase aluminum oxide powder involves adding aluminum hydroxide, α-phase aluminum oxide seed crystal and calcining additive in a grinder, grinding, mixing uniformly to obtain a mixed material, adding the mixed material into a crucible, placing in a tubular furnace, raising the temperature to a calcining temperature of 600-1000℃ at a heating rate of 5-10℃/minute under an inert atmosphere, replacing the inert gas with oxygen, calcining at high temperature for 5-30 minutes, naturally cooling to room temperature, and discharging. The calcining additive comprises one or more of carbon black, graphene, carbon nanotube and gas-phase growth carbon fiber, and has a specific surface area of 10-500 m2/g. USE - Low-temperature preparation of α-phase aluminum oxide powder used for preparing high-grade refractory flame-retardant material, fine ceramic, battery separator material and precise polishing material. ADVANTAGE - The method is simple, easy, environmentally-friendly and economical, prevents irregular shape and uneven size of aluminum oxide, uses wide raw material source, and ensures excellent repeatability and low calcining temperature.