• 专利标题:   Improving quality of metal catalytic thin layer prepared by sputtering comprises cleaning Si/SiO2 substrate, photoetching the pattern, sputtering a layer of metal thin layer with the graphene of catalyzing and growing on the substrate sheet by using the sputtering table, peeling and etching.
  • 专利号:   CN115928042-A
  • 发明人:   ZHAO Y, YU X, LIU Z, NIE X, SONG Z, DENG J, HE X
  • 专利权人:   UNIV BEIJING TECHNOLOGY
  • 国际专利分类:   C01B032/186, C23C016/01, C23C016/02, C23C016/26, C30B023/00, C30B029/02, C30B033/04, C30B033/12, H01L021/02
  • 专利详细信息:   CN115928042-A 07 Apr 2023 C23C-016/26 202341 Chinese
  • 申请详细信息:   CN115928042-A CN11435828 16 Nov 2022
  • 优先权号:   CN11435828

▎ 摘  要

NOVELTY - Improving quality of metal catalytic thin layer prepared by sputtering comprises (1) cleaning Si/SiO2 substrate; (2) photoetching the pattern; (3) sputtering a layer of metal thin layer with the graphene of catalyzing and growing on the substrate sheet by using the sputtering table; (4) peeling, obtaining the patterned sputtering metal thin layer; (5) etching the sputtered metal, introducing mixed gas Ar: SiCl4 into the reaction chamber, setting radio frequency RF power and ICP powe, (6) using multitemperature area CVD growth graphene the patterned metal catalytic thin layer, finishing the growth of graphene in the third temperature zone of the threetemperature zone tubular furnace, introducing argon gas to wash the chamber, introducing hydrogen into the chamber, heating under the pure hydrogen atmosphere, finishing the growth of the graphene under the condition of the chamber pressure of 770Pa and etching the metal catalytic thin layer to obtain the insitu patterned graphene. USE - The method is useful for improving quality of metal catalytic thin layer prepared by sputtering.