• 专利标题:   Preparing graphene composite material involves adding graphene oxide into deionized water, ultrasonically dispersing to obtain oxidized graphene suspension, mixing graphene oxide suspension with prepared silver ammonia solution.
  • 专利号:   CN107445145-A
  • 发明人:   LU W
  • 专利权人:   ZHANGJIAGANG HUIDING NEW MATERIAL TECHNO
  • 国际专利分类:   C01B032/184, G01N021/65
  • 专利详细信息:   CN107445145-A 08 Dec 2017 C01B-032/184 201804 Pages: 5 Chinese
  • 申请详细信息:   CN107445145-A CN10676745 09 Aug 2017
  • 优先权号:   CN10676745

▎ 摘  要

NOVELTY - Preparing graphene composite material involves adding graphene oxide into deionized water, ultrasonically dispersing for 1-2 hours to obtain oxidized graphene suspension, mixing graphene oxide suspension with prepared silver ammonia solution in ratio 5:1, and stirring for 30-60 minutes. The organic reducing agent is added, and pH is adjusted 10-12. The mixture is stirred at 80-90 degrees C in water bath for 2-3 hours, and subjected to magnetic force at 45-60 degrees C. The mixture is cooled, filtered, washed with ethanol and de-ionized water for 3-5 times. USE - Method for preparing graphene composite material (claimed). ADVANTAGE - The method enables to prepare graphene composite material that has good Raman enhancement effect, and in simple manner. DETAILED DESCRIPTION - Preparing graphene composite material involves adding graphene oxide into deionized water, ultrasonically dispersing for 1-2 hours to obtain oxidized graphene suspension, mixing graphene oxide suspension with prepared silver ammonia solution in ratio 5:1, and stirring for 30-60 minutes. The organic reducing agent is added, and pH is adjusted 10-12. The mixture is stirred at 80-90 degrees C in water bath for 2-3 hours, and subjected to magnetic force at 45-60 degrees C. The mixture is cooled, filtered, washed with ethanol and de-ionized water for 3-5 times, dried at 40-60 degrees C for 10-12 hours to obtain silver-graphite composite material.