• 专利标题:   Preparing graphene-supported cobalt disulfide particle composite material useful for catalytic electrolysis of water, comprises dispersing graphene in water, adding cobalt acetate and carbon disulfide, stirring and hydrothermally processing.
  • 专利号:   CN108927177-A
  • 发明人:   HAN X, MA X, HU W, DENG Y, ZHONG C
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   B01J027/043, B01J035/02, C25B001/04, C25B011/06
  • 专利详细信息:   CN108927177-A 04 Dec 2018 B01J-027/043 201908 Pages: 10 Chinese
  • 申请详细信息:   CN108927177-A CN10573912 06 Jun 2018
  • 优先权号:   CN10573912

▎ 摘  要

NOVELTY - Preparing graphene-supported cobalt disulfide particle composite material comprises (i) uniformly dispersing graphene in water to obtain suspension; (ii) adding cobalt acetate tetrahydrate into the suspension and mechanically stirring at room temperature; (iii) adding ethylenediamine into the suspension and mechanically stirring at room temperature; (iv) adding carbon disulfide to the suspension and mechanically stirring at room temperature; (v) pouring the mixture into polytetrafluoroethylene lined reaction kettle, placing the reaction kettle in an oven and carrying out hydrothermal treatment; and (vi) washing the sample using water for three times, centrifuging, collecting product and freeze-drying. USE - The composite material is useful for catalytic electrolysis of water (claimed). ADVANTAGE - The method is simple, suitable for industrial production and convenient to operate, and has controllable conditions and high repeatability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene-supported cobalt disulfide particle composite material prepared by the above method, comprising a pure cobalt disulfide phase uniformly distributed on the graphene, where the particle size of cobalt disulfide is 70-200 nm.