• 专利标题:   Mercaptopropionic acid/2-(3,4-epoxycyclohexyl)ethyltrimethoxysilane/reduced graphene oxide reinforced aqueous epoxy amino baking varnish comprises aqueous epoxy emulsifier, epoxy resin, amino resin, reinforcing agent, defoamer, and water.
  • 专利号:   CN112980296-A, CN112980296-B
  • 发明人:   ZHENG Y, ZENG H
  • 专利权人:   UNIV FUZHOU
  • 国际专利分类:   C08F220/20, C08F283/10, C09D161/20, C09D163/00, C09D005/08, C09D007/62, C09D007/65
  • 专利详细信息:   CN112980296-A 18 Jun 2021 C09D-163/00 202164 Pages: 11 Chinese
  • 申请详细信息:   CN112980296-A CN10350686 31 Mar 2021
  • 优先权号:   CN10350686

▎ 摘  要

NOVELTY - A mercaptopropionic acid/KH-567 (RTM: 2-(3,4-epoxycyclohexyl)ethyltrimethoxysilane)/reduced graphene oxide reinforced aqueous epoxy amino baking varnish comprises 10-15 pts. wt. aqueous epoxy emulsifier, 30-50 pts. wt. epoxy resin, 35-40 pts. wt. amino resin, 0.5-2 pts. wt. reinforcing agent, 0.1-0.5 pt. wt. defoamer, and 40-70 pts. wt. deionized water. The aqueous epoxy emulsifier is obtained by dissolving epoxy resin E-44 in a solvent, adding N,N-methylenebisacrylamide, reacting with the epoxy resin, adding hydroxyethyl acrylate and a little potassium persulfate as initiator, heating and stirring to make the hydroxyethyl acrylate generate free radical polymerization, and obtaining an epoxy resin-ethyl polyacrylate as the aqueous epoxy emulsifier. USE - Mercaptopropionic acid/KH-567 (RTM: 2-(3,4-epoxycyclohexyl)ethyltrimethoxysilane)/reduced graphene oxide reinforced aqueous epoxy amino baking varnish. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of the varnish, which involves dispersing the epoxy resin and reinforcing agent at 1000 rpm, adding the aqueous epoxy emulsifier, slowly dripping deionized water to finish reverse rotation, preparing into an aqueous epoxy emulsion, mixing the aqueous epoxy emulsion, amino resin, and deionized water, adding defoamer, and dispersing for 30 minutes at 1500 rpm.