▎ 摘 要
NOVELTY - Preparing acid chlorinated graphene oxide modified polyamide reverse osmosis membrane with antibacterial property comprises e.g. dissolving polyfunctional aromatic amine compound in water, soaking support layer in aqueous solution, soaking product in 0.02-2 wt.% oil phase solution, adding polyfunctional acid chloride solution in organic solvent, removing excess oil phase solution from the surface, evaporating oil phase solution, uniformly mixing graphene and thionyl chloride solution in isoparaffin solvent in a pressure of -0.1 to -0.03 Mpa, carrying out rotary evaporation of thionyl chloride. USE - The acid chlorinated graphene oxide modified polyamide reverse osmosis membrane is useful for treating water (claimed). ADVANTAGE - The acid chlorinated graphene oxide modified polyamide reverse osmosis membrane has water flux rate, and high salt rejection rate. DETAILED DESCRIPTION - Preparing acid chlorinated graphene oxide modified polyamide reverse osmosis membrane with antibacterial property comprises (i) dissolving polyfunctional aromatic amine compound in water, to obtain 0.1-10 wt.% aqueous solution, soaking support layer in aqueous solution, removing excess aqueous solution on surface of support layer; (ii) soaking the step (i) product in 0.02-2 wt.% oil phase solution, adding polyfunctional acid chloride solution in organic solvent, removing excess oil phase solution from the surface, evaporating oil phase solution, to obtain unmodified reverse osmosis membrane; (iii) uniformly mixing 0.1-5 g/l graphene and 0.1-1 g/l thionyl chloride solution in isoparaffin solvent in a pressure of -0.1 to -0.03 Mpa, carrying out rotary evaporation of thionyl chloride at 50-80 degrees C, to obtain acid chlorinated graphene oxide modifier, uniformly coating acid chlorinated graphene oxide modifier on step (ii) obtained reverse osmosis membrane, allowing to stand for 120-1200 seconds, removing the excess modifier, where the graphene is monolayer; and (iv) drying step (iii) obtained reverse osmosis membrane at 60-100 degrees C for 80-600 seconds, to obtain the final product.