• 专利标题:   Preparation of graphene by placing graphene oxide solution in glass container, placing electrode in solution, powering on direct-current voltage-stabilizing power supply, and electrochemically reducing.
  • 专利号:   CN102181877-A
  • 发明人:   ZHANG D, ZHU P
  • 专利权人:   UNIV TONGJI
  • 国际专利分类:   C25B001/00
  • 专利详细信息:   CN102181877-A 14 Sep 2011 C25B-001/00 201174 Pages: 8 Chinese
  • 申请详细信息:   CN102181877-A CN10103554 25 Apr 2011
  • 优先权号:   CN10103554

▎ 摘  要

NOVELTY - Preparation of graphene comprises dissolving graphene oxide in deionized water, and ultrasonically stripping to obtain graphene oxide solution; placing the solution in a glass container; connecting a negative electrode material and a positive electrode material with one end of a copper wire, placing the electrode in the solution, and connecting the other end of the copper guide wire with a negative electrode and a positive electrode of a direct-current voltage-stabilizing power supply; and powering on the power supply, and electrochemically reducing for 1-60 minutes. USE - Method for the preparation of graphene (claimed). ADVANTAGE - The method produces high quality graphene. It is simple and convenient, inexpensive, safe, and environment friendly. DETAILED DESCRIPTION - Preparation of graphene comprises: (A) dissolving graphene oxide with particle size of 25-140 mu m in deionized water, and ultrasonically stripping to obtain 5-10 mg/mL graphene oxide solution; (B) placing the graphene oxide solution in a glass container; (C) connecting a negative electrode material and a positive electrode material with one end of a copper wire, placing the electrode in the graphene oxide solution, and connecting the other end of the copper guide wire with a negative electrode and a positive electrode of a direct-current voltage-stabilizing power supply; and (D) powering on the power supply, controlling voltage at 10-50 V, controlling temperature at 25-90 degrees C, and electrochemically reducing for 1-60 minutes.