• 专利标题:   Preparing graphene oxide loaded nano titanium dioxide used for preparation of photocatalytic graphene antibacterial fiber, involves adding water into graphene oxide for ultrasonic treatment, mixing graphene oxide dispersion liquid with ethanol, adjusting pH, reacting, centrifuging, cleaning, drying.
  • 专利号:   CN114600904-A
  • 发明人:   YUAN K, ZHANG W, LI M, CHEN Y, WANG Y, ZHANG L, CHEN L
  • 专利权人:   BEIJING INNOVATION AIKA TECHNOLOGY CO
  • 国际专利分类:   A01N059/00, A01P001/00, A01P003/00, B01J021/18, D01F001/10, D01F006/92
  • 专利详细信息:   CN114600904-A 10 Jun 2022 A01N-059/00 202272 Chinese
  • 申请详细信息:   CN114600904-A CN10226737 09 Mar 2022
  • 优先权号:   CN10226737

▎ 摘  要

NOVELTY - Preparing graphene oxide loaded nano titanium dioxide involves adding water into graphene oxide for ultrasonic treatment to obtain 2-3.5 g/L graphene oxide dispersion liquid; mixing graphene oxide dispersion liquid with ethanol, and adjusting pH to 2-3 to obtain 15-25 vol.% reaction solution; mixing tetrabutyl titanate and ethanol to prepare 75-85 vol.% reaction precursor; dropwise adding reaction precursor into reaction solution at temperature of 75-85℃, and continuously reacting for 20-30 hours at temperature of 78-82℃ to obtain suspension; centrifuging, cleaning and drying turbid liquid to obtain graphene oxide loaded nano titanium dioxide. USE - Method for preparing graphene oxide loaded nano titanium dioxide used for preparation of photocatalytic graphene antibacterial fiber (claimed). ADVANTAGE - The method helps in improving antibacterial property of material, where nano titanium dioxide is more uniformly distributed on graphene oxide, and is not easy to fall off; provides more durable antibacterial effect. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: (1) a photocatalytic graphene antibacterial fiber, which comprises polyester resin powder, and 0.3-2 wt.% graphene oxide-loaded nano titanium dioxide; (2) a method for preparing photocatalytic graphene antibacterial fiber, which involves: (a) mixing polyester resin powder and graphene oxide loaded nano titanium dioxide powder; (b) granulating and spinning to obtain photocatalytic graphene antibacterial fiber.