• 专利标题:   Preparation of graphene film used as super capacitor includes adding graphite oxide to organic solvent, adding dispersant, ultrasonic treating, adding hydrazine, reacting, filtering, drying, peeling and heating.
  • 专利号:   CN103578771-A
  • 发明人:   WANG Y, WU F, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   C01B031/04, H01G009/04, H01M004/66
  • 专利详细信息:   CN103578771-A 12 Feb 2014 H01G-009/04 201432 Pages: 6 Chinese
  • 申请详细信息:   CN103578771-A CN10248651 18 Jul 2012
  • 优先权号:   CN10248651

▎ 摘  要

NOVELTY - Preparation of graphene film comprises adding graphite oxide to organic solvent, ultrasonic treating for 0.5-1 hour, adding dispersant comprising fluorine-containing sulfonated polyaryl ether ketone solution or fluorine-containing sulfonated polyaryl ether sulfone solution, ultrasonic treating for 0.5-1 hour to obtain graphene oxide suspension, adding hydrazine hydrate, reacting at 100 degrees C for 12-24 hours, filtering using microporous membrane vacuum filtration, drying cake at 40-60 degrees C, peeling off membrane and heat treating crude product in oven at 150-250 degrees C for 0.5-2 hours. USE - Method for preparing graphene film used as super capacitor and current collector of lithium-ion battery (all claimed). ADVANTAGE - The method is simple and easy to control. The graphene film with 1-10 mu m thickness is light, uniform, and strongly conductive.