• 专利标题:   Fabricating acetylene-benzoxazine functionalized particles comprises adding particles to alkaline solution, stirring solution to cause particles to acquire hydroxyl groups producing activated particles, adding acetylene benzoxazine into solvent solution, and drying product.
  • 专利号:   EP4148030-A1, CA3172613-A1, US2023069939-A1, JP2023039416-A
  • 发明人:   IFTIME G, WEI J, CHINTAPALLI M
  • 专利权人:   PALO ALTO RES CENT INC, PALO ALTO RES CENT INC, PALO ALTO RES CENT INC
  • 国际专利分类:   C04B035/628, C08G073/00, C04B014/32, C08K003/14, C08K009/04, B33Y010/00, B33Y070/10, C01B032/956, C09C001/28, C09C003/08
  • 专利详细信息:   EP4148030-A1 15 Mar 2023 C04B-035/628 202323 Pages: 15 English
  • 申请详细信息:   EP4148030-A1 EP191549 22 Aug 2022
  • 优先权号:   US241698P, US854261

▎ 摘  要

NOVELTY - Method comprises adding particles to an alkaline solution, stirring the solution to cause the particles to acquire hydroxyl groups producing activated particles, dispersing the activated particles into a solvent solution, adding acetylene benzoxazine into the solvent solution, mixing the solvent solution, removing the solvent from the solvent solution to produce acetylene-benzoxazine functionalized particles, and drying the acetylene-benzoxazine functionalized particles. USE - The method is used for fabricating acetylene-benzoxazine functionalized particles, which is used in ceramic matrix composites. ADVANTAGE - The method fabricates acetylene-benzoxazine functionalized particles in one-step process, eliminates the need to separate and purify particles, then remixing them with benzoxazine monomer, produces high yield char upon pyrolysis, allows for radical polymerization of the acetylene groups to produce dense and mechanically strong silicon carbide/benzoxazine composites upon curing, and increases the high-temperature stability of the cured object made with these formulations. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a composition of matter, comprising acetylene-benzoxazine functionalized particles dispersed in a resin, optionally where the functionalized particles comprise silicon carbide and the resin comprises a benzoxazine resin.