• 专利标题:   Preparation of graphene, by mixing N-methylpyrrolidone and graphite powder, dispersing in water bath, grinding in ball mill together with alumina balls, crushing, adding deionized water, ultrasonically-dispersing and drying in oven.
  • 专利号:   CN106115679-A
  • 发明人:   ZHANG L, WANG Z, LI Q, SHI G, WU J, LI Y, LIU M, XU H
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN106115679-A 16 Nov 2016 C01B-031/04 201701 Pages: 8 Chinese
  • 申请详细信息:   CN106115679-A CN10513161 04 Jul 2016
  • 优先权号:   CN10513161

▎ 摘  要

NOVELTY - Preparation of graphene involves mixing N-methylpyrrolidone and graphite powder, dispersing in water bath to form paste solution, grinding in ball mill together with alumina balls, placing ball mill on planetary ball mill, crushing, adding deionized water, ultrasonically-dispersing in water bath, washing residual N-methylpyrrolidone deionized water and drying in oven to obtain resulting black powder, which is multilayered graphene. USE - Preparation of graphene (claimed). ADVANTAGE - The method enables simple and economical preparation of graphene using simple organic solvent. DETAILED DESCRIPTION - Preparation of graphene involves mixing N-methylpyrrolidone and graphite powder in a mass ratio 1-5:1, dispersing in water bath at 60 degrees C for half an hour to form a paste solution, grinding in ball mill together with alumina balls, placing ball mill on a planetary ball mill, adjusting rotational speed of ball mill to 350-450 rpm, crushing for 12-24 hours, adding deionized water, ultrasonically-dispersing in water bath, stirring constantly, washing residual N-methylpyrrolidone thoroughly with deionized water and drying in oven to completely remove liquid phase and obtain resulting black powder, which is multilayered graphene. The mass ratio of alumina ball, graphite powder and N-methylpyrrolidone is 1:1-50:10-20. The mass ratio of deionized water and graphite powder is 1-2:1.