• 专利标题:   Preparing high quality graphene comprises e.g. adding natural graphite powder to reactor filled with ammonia gas, then adding sodium metal and liquid ammonia into reaction vessel to obtain mixed liquid and heating.
  • 专利号:   CN108314021-A
  • 发明人:   SUN L, MA Y, LI D, LIANG S
  • 专利权人:   SHANDONG HENGHUA NEW MATERIALS CO LTD
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN108314021-A 24 Jul 2018 C01B-032/19 201853 Pages: 8 Chinese
  • 申请详细信息:   CN108314021-A CN10032362 16 Jan 2017
  • 优先权号:   CN10032362

▎ 摘  要

NOVELTY - Preparing high quality graphene comprises (i) adding natural graphite powder to reactor filled with ammonia gas, (ii) adding sodium metal and liquid ammonia into reaction vessel of step (i) to obtain mixed liquid, (iii) heating the reaction vessel of step (ii) until the liquid ammonia is evaporated to obtain sodium intercalated graphite powder, (iv) adding the sodium intercalated graphite powder into stripper and adding water to reacting, and (v) washing the material obtained in step (iv) with water, filtering and drying to obtain graphene product. USE - The method is useful for preparing high quality graphene. ADVANTAGE - The method: utilizes natural graphite powder as a raw material.