• 专利标题:   Preparation of graphene foam composite material loaded with magnetic hollow nanospheres includes preparing graphene oxide with different oxidation degree, mixing graphene oxide powder and isopropanol and performing hydrothermal reaction.
  • 专利号:   CN110564365-A
  • 发明人:   CHEN P, LIU J, XU D, YU Q, CHEN B
  • 专利权人:   UNIV DALIAN TECHNOLOGY
  • 国际专利分类:   C09K003/00, H01F001/00
  • 专利详细信息:   CN110564365-A 13 Dec 2019 C09K-003/00 202003 Pages: 10 Chinese
  • 申请详细信息:   CN110564365-A CN10826320 03 Sep 2019
  • 优先权号:   CN10826320

▎ 摘  要

NOVELTY - Preparation of graphene foam composite material loaded with magnetic hollow nanospheres comprises preparing graphene oxide with different oxidation degree by Hummers method, freeze-drying to obtain graphene oxide powder, mixing graphene oxide powder and isopropanol, adding metal salt, cetrimonium bromide (CTAB), glycerin and water, placing in ultrasonic 1-2 hours, mixing to obtain reaction liquid, injecting reaction fluid into the kettle, performing hydrothermal reaction at 160-220 degrees C for 6-24 hours, separating, washing, freeze-drying to obtain precursor of graphene foam with metal salt and calcining at high temperature under the condition of inert gas. The proportion of each substance in the reaction solution is graphene oxide powder, isopropanol, glycerin, water, CTAB and metal salt at 100-400 mg: 50-70 ml: 7-10 ml: 0-2 ml: 0-2000 mg: 500-3000 mg. USE - The method is for preparation of graphene foam composite material loaded with magnetic hollow nanospheres. ADVANTAGE - The composite material has excellent electromagnetic performance.