• 专利标题:   Preparing graphene nanocomposite material involves weighing bisphenol A diglycidyl ether, diethyl toluene diamine, modified graphene oxide, absolute ethanol, mixing bisphenol A diglycidyl ether and diethyltoluenediamine.
  • 专利号:   CN111763406-A
  • 发明人:   CHU K, TIAN Y, GUO Y, WEI Z, QU W
  • 专利权人:   UNIV LANZHOU JIAOTONG
  • 国际专利分类:   B82Y030/00, B82Y040/00, C08K013/06, C08K003/04, C08K003/36, C08K009/04, C08K009/06, C08K009/12, C08L063/02
  • 专利详细信息:   CN111763406-A 13 Oct 2020 C08L-063/02 202097 Pages: 8 Chinese
  • 申请详细信息:   CN111763406-A CN10778444 05 Aug 2020
  • 优先权号:   CN10778444

▎ 摘  要

NOVELTY - Preparing graphene nanocomposite material involves weighing 50-60 pts. wt. bisphenol A diglycidyl ether, 11-14 pts. wt. diethyl toluene diamine, 2-3 pts. wt. modified graphene oxide, 100 pts. wt. absolute ethanol, mixing bisphenol A diglycidyl ether and diethyltoluenediamine, stirring at 100 degrees C for 15-18 minutes to obtain a light yellow liquid epoxy resin pre-compound, adding the epoxy resin premix to absolute ethanol, stirring and mixing at 300r/minutes for 26-30 minutes at room temperature, placing in a vacuum oven at 110 degrees C to degas for 30-40 minutes to obtain epoxy resin mixture of pre-compound and ethanol, adding the modified graphene oxide to the mixture of the epoxy resin pre-composite and ethanol, and ultrasonically treating for 40-50 minutes at room temperature to form a suspension, placing the suspension in a vacuum oven at 110 degrees C for degassing 30-40 minutes to obtain a mixture, pouring the mixture into a mold. USE - Method for preparing graphene nanocomposite material. ADVANTAGE - The method enables to prepare graphene nanocomposite material has excellent flame retardant property and improves the mechanical property and heat-resistant stability of the composite material. DETAILED DESCRIPTION - Preparing graphene nanocomposite material involves weighing 50-60 pts. wt. bisphenol A diglycidyl ether, 11-14 pts. wt. diethyl toluene diamine, 2-3 pts. wt. modified graphene oxide, 100 pts. wt. absolute ethanol, mixing bisphenol A diglycidyl ether and diethyltoluenediamine, stirring at 100 degrees C for 15-18 minutes to obtain a light yellow liquid epoxy resin pre-compound, adding the epoxy resin premix to absolute ethanol, stirring and mixing at 300r/minutes for 26-30 minutes at room temperature, placing in a vacuum oven at 110 degrees C to degas for 30-40 minutes to obtain epoxy resin mixture of pre-compound and ethanol, adding the modified graphene oxide to the mixture of the epoxy resin pre-composite and ethanol, and ultrasonically treating for 40-50 minutes at room temperature to form a suspension, placing the suspension in a vacuum oven at 110 degrees C for degassing 30-40 minutes to obtain a mixture, pouring the mixture into a mold, solidifying according to a stepped heating method, demolding, and cooling to room temperature naturally to obtain a composite material.