• 专利标题:   Preparing graphene oxide modified metal sulfide composite photocatalyst by milling pyrite, washing with ultrapure water, drying in freeze dryer, and treating graphene oxide in ultrasonic water bath, adding pyrite, grinding and air drying.
  • 专利号:   CN110918102-A
  • 发明人:   SHU X, LI C, ZHANG W, PENG Q, DU H, TIAN W, LIN H
  • 专利权人:   UNIV GUILIN TECHNOLOGY
  • 国际专利分类:   B01J027/043, C02F001/30, C02F101/30, C02F101/38
  • 专利详细信息:   CN110918102-A 27 Mar 2020 B01J-027/043 202033 Pages: 6 Chinese
  • 申请详细信息:   CN110918102-A CN11258790 10 Dec 2019
  • 优先权号:   CN11258790

▎ 摘  要

NOVELTY - Method for preparing graphene oxide modified metal sulfide composite photocatalyst involves (a) milling pyrite with a ball mill for 5 minutes, passing through a 100 mesh sieve, washing 6 times with ultrapure water in a volume ratio of 1:5, placing in a freeze dryer to dry for 48 hours, and (b) taking graphene oxide with ultrapure water to 12 mg/ml in a ultrasonic water bath at a temperature of 40-45 degrees C for 30 minutes, taking 1 ml, adding 0.2 g pyrite, grinding with mortar for 5 minutes, putting in a fume hood and air drying to get the composite photocatalyst. USE - The method is used for preparing graphene oxide modified metal sulfide composite photocatalyst which is used in photocatalytic degradation of rhodamine dye in wastewater. ADVANTAGE - The method provides excellent photocatalytic activity than pure pyrite catalyst, and has degradation rate increased by 64%.