• 专利标题:   Manufacturing graphene skeleton moxibustion paste, comprises e.g. using a single diameter of carbon fiber knitted with a fishing net needle method into a layer structure of the network, controlling cell gap, and knitting.
  • 专利号:   CN107334633-A, CN107334633-B
  • 发明人:   HE H, SONG J
  • 专利权人:   QINGDAO ZHUOHU MEDICAL SUPPLIES CO LTD
  • 国际专利分类:   A61H039/06, A61L031/14
  • 专利详细信息:   CN107334633-A 10 Nov 2017 A61H-039/06 201779 Pages: 6 Chinese
  • 申请详细信息:   CN107334633-A CN10546372 06 Jul 2017
  • 优先权号:   CN10546372

▎ 摘  要

NOVELTY - Manufacturing graphene skeleton moxibustion paste, comprises e.g. using a single diameter of carbon fiber knitted with a fishing net needle method into a layer structure of the network, controlling cell gap, when knitting, every three layers and five layers are taken as a composition layer, to obtain three composition carbon fiber webs with two empty packages, taking carbon fiber network, placing under aerobic environment, keeping, to obtain pre-oxidized carbon fiber web, taking the pre-oxidized carbon fiber web, and slowly immersing in concentrated sulfuric acid, obtaining the first mixture. USE - The method is useful for manufacturing graphene skeleton moxibustion paste (claimed). ADVANTAGE - The graphene skeleton has good compatibility, long lasting time, and can recycling the product. DETAILED DESCRIPTION - Manufacturing graphene skeleton moxibustion paste, comprises (i) (a) using a single diameter of 5-7 mu m carbon fiber knitted with a fishing net needle method into a 9-15 layer structure of the network, controlling cell gap is 0.1-0.3 mm, when knitting, every three layers and five layers are taken as a composition layer, to obtain three composition carbon fiber webs with two empty packages, (b) taking carbon fiber network, placing at 550-600 degrees C under aerobic environment, keeping for 3-3.5 hours, to obtain pre-oxidized carbon fiber web, (c) taking the pre-oxidized carbon fiber web obtained in step (b), slowly immersing in concentrated sulfuric acid in a concentration of 98%, obtaining the first mixture, (d) taking the first mixture obtained in step (c), slowly adding in to the total mass of raw carbon fiber for 5-6 times into potassium permanganate powder, and slowly stirring with a glass rod, sustaining for 2-3 hours, to Obtain a second mixture, (e) slowly placing the container containing of the second mixture into the ice water tub, keeping the container in opening above the ice water level, and placing in the container of mercury thermometer; (vi) slowly adding drop-wise purified water into the second mixture, adding speed control in the container liquid temperature is not greater than 40 degrees C, dropping the total volume of the second mixture of the total volume of 2-2.5 times, to obtain a third mixture, (f) adding third mixed solution in drop-wise into a volume fraction of 3-5% aqueous hydrogen peroxide, to the third mixed liquid no bubble generation, filtering out the liquid, to obtain fully oxidized graphite oxide, (g) taking the obtained graphite oxide in step (f), immersing in purified water, slowly heating at 50-60 degrees C, continuously adding vitamin C powder to the end of the reaction, filtering liquid, obtaining after purification there are two empty package of graphene skeleton, where the two empty packages are a first empty package and a second empty package; and (ii) choosing the fresh folium artemisiae argyi of 3-5 years, obtaining wormwood, mechanically crushing the wormwood into powder of size 0.5-2mm, filling the second empty packet, where the first empty is filling with grain diameter 0.5-1.5 mm of quicklime, and the first empty the sticking rectangle film away from the outer surface of the second air bag.