• 专利标题:   Preparing 5-hydroxymethylfurfural by sulfonated graphen solid acid catalytic fructose dehydration, involves contacting ionic liquid and auxiliary agent, adding sulfonated graphene to mixed solvent, and treating in microwave power.
  • 专利号:   CN106905270-A
  • 发明人:   JU M, LI W, HOU Q, WANG Y, TUERHONG M, WANG J
  • 专利权人:   UNIV NANKAI, UNIV KASHGAR
  • 国际专利分类:   B01J027/02, C07D307/46
  • 专利详细信息:   CN106905270-A 30 Jun 2017 C07D-307/46 201763 Pages: 6 Chinese
  • 申请详细信息:   CN106905270-A CN10155294 16 Mar 2017
  • 优先权号:   CN10155294

▎ 摘  要

NOVELTY - Preparing 5-hydroxymethylfurfural by sulfonated graphen solid acid catalytic fructose dehydration, involves contacting ionic liquid and auxiliary agent, adding 0.5-1.5 pts. wt. of sulfonated graphene to 100 pts. wt. of the mixed solvent, and treating in microwave power of 200-800 Watt and for 10-60 minutes. 5-25 pts. wt. of fructose is added to the system, and heated to 100-140 degrees C for 30-180 minutes. The catalyst is recovered by centrifugation after the completion of the reaction. The solution is extracted and distilled to obtain 5-hydroxymethylfurfural. USE - Method for preparing 5-hydroxymethylfurfural (claimed). ADVANTAGE - The method enables to prepare 5-hydroxymethylfurfural in a simple and highly efficient manner that has economic feasibility.