• 专利标题:   Preparation of graphene by adding graphite powder to tetrahydrofuran solution and obtaining graphite-powder tetrahydrofuran dispersion liquid, adding halogenated organic reagent, reacting, washing and drying.
  • 专利号:   CN103058182-A, CN103058182-B
  • 发明人:   FENG L, LIU Y, XIE S, ZHENG L, DENG S, HUANG R
  • 专利权人:   UNIV XIAMEN
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103058182-A 24 Apr 2013 C01B-031/04 201372 Pages: 9 Chinese
  • 申请详细信息:   CN103058182-A CN10031362 27 Jan 2013
  • 优先权号:   CN10031362

▎ 摘  要

NOVELTY - Preparing graphene comprises adding graphite powder to a tetrahydrofuran solution and obtaining graphite-powder tetrahydrofuran dispersion liquid by carrying out ultrasonic dispersion under the protection of nitrogen gas; adding alkali metal and naphthalene to the dispersion liquid, stirring under the protection of the nitrogen gas to obtain the mixed solution; adding halogenated organic reagent to the mixed solution, and reacting under the protection of the nitrogen gas to obtain a solid product; and washing and drying the solid product to obtain the graphene powder. USE - Method for preparing graphene (claimed). ADVANTAGE - The method has low cost and low device requirements, and is simple, easy and good for industrial production.