• 专利标题:   Large-area graphene and manufacturing method thereof capable of obtaining graphene having a diameter value between 1 less than mu greater than m and 50 less than mu greater than m obtained by a Raman spectroscopy.
  • 专利号:   TW201825395-A
  • 发明人:   SONG J, LIU J, WANG G, WANG H, WANG S, ZANG P, LIN Y, LIN H
  • 专利权人:   HENAN GRAPHENE SYNTHETIC CO LTD
  • 国际专利分类:   C01B032/20
  • 专利详细信息:   TW201825395-A 16 Jul 2018 C01B-032/20 201902 Pages: 0 Chinese
  • 申请详细信息:   TW201825395-A TW100961 12 Jan 2017
  • 优先权号:   TW100961

▎ 摘  要

NOVELTY - A manufacturing method of graphene comprises the following steps: providing a substrate and disposing a carbon source on the substrate, wherein the substrate is made of cobalt or nickel; placing the substrate in a heating furnace, wherein the heating furnace provides a heating temperature between 1000 DEG C and 1300 DEG C and an atmosphere environment for a predetermined period of time so as to allow the carbon source to permeate the substrate; and continuously cooling the heating furnace at a cooling rate between 0.1 DEG C/min and 5 DEG C/min so as to enable the carbon source permeating the substrate to be recrystallized for precipitating the graphene attached onto the substrate. The growth rate of the graphene is increased at a low cooling rate between 0.1 DEG C/min and 5 DEG C/min, and the graphene obtained after the process is finished has a diameter value (La) between 1 less than mu greater than m and 50 less than mu greater than m obtained by a Raman spectroscopy.