• 专利标题:   Preparation of graphene oxide/silver nanocomposite hybrid antibacterial material used for functionalizing fiber or fabric product, involves using graphene oxide aqueous solution, strong alkali solution, epichlorohydrin and deionized water.
  • 专利号:   CN112806389-A, CN112806389-B
  • 发明人:   ZHANG R, ZHANG D, CHEN Y, ZHU B, LIN H, YAN Y
  • 专利权人:   UNIV SOOCHOW
  • 国际专利分类:   A01N025/08, A01N059/00, A01N059/16, A01P001/00, A01P003/00, D06M011/74, D06M011/83
  • 专利详细信息:   CN112806389-A 18 May 2021 A01N-059/16 202154 Pages: 11 Chinese
  • 申请详细信息:   CN112806389-A CN10136912 01 Feb 2021
  • 优先权号:   CN10136912

▎ 摘  要

NOVELTY - Preparation of graphene oxide/silver nanocomposite hybrid antibacterial material involves adjusting the pH of the graphene oxide aqueous solution to alkaline with a strong alkali solution, adding epichlorohydrin to alkaline graphene oxide aqueous solution, stirring and reacting at 50-70 degrees C for 2-5 hours, after cooling, using deionized water for centrifugal washing 3-5 times to obtain epichlorohydrin-modified graphene oxide, dispersing epichlorohydrin-modified graphene oxide in the carbonate buffer solution at a concentration of 0.3-3 g/l, mixing the amino-terminated hyperbranched polymer solution with the silver nitrate solution and heating it to boiling for 3-5 minutes, adding the amino-terminated hyperbranched polymer nano-silver solution to the epichlorohydrin modified graphene oxide solution, stirring, and reacting at 50-70 degrees C for 2-5 hours. USE - Preparation of graphene oxide/silver nanocomposite hybrid antibacterial material used for functionalizing fiber or fabric product (claimed). ADVANTAGE - The method is simple, and enables preparation of graphene oxide/silver nanocomposite hybrid antibacterial material. The prepared graphene oxide/silver nanocomposite hybrid antibacterial material provides functionalized fiber or fabric product with excellent antibacterial effect and antiviral effect. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) graphene oxide/silver nanocomposite hybrid antibacterial material, which is prepared by the method; (2) use of the graphene oxide/silver nanocomposite hybrid antibacterial material in the fiber/fabric which is subjected to padding assembly finishing in a finishing solution obtained from the graphene oxide/silver nanocomposite hybrid antibacterial material; and (3) fiber or fabric product, which comprises graphene oxide/silver nanocomposite hybrid antibacterial material.